ES466943A1 - Procedimiento para la preparacion de trans-ciclohexan-1,4- diisocianato, transciclohexan,1,4-diamina,trans-ciclohexan- 1,4-diuretanos, trans-ciclohexan 1,4-diureas o de trans-ci- clohexan-1,4-disulfonilureas. - Google Patents
Procedimiento para la preparacion de trans-ciclohexan-1,4- diisocianato, transciclohexan,1,4-diamina,trans-ciclohexan- 1,4-diuretanos, trans-ciclohexan 1,4-diureas o de trans-ci- clohexan-1,4-disulfonilureas.Info
- Publication number
- ES466943A1 ES466943A1 ES466943A ES466943A ES466943A1 ES 466943 A1 ES466943 A1 ES 466943A1 ES 466943 A ES466943 A ES 466943A ES 466943 A ES466943 A ES 466943A ES 466943 A1 ES466943 A1 ES 466943A1
- Authority
- ES
- Spain
- Prior art keywords
- cyclohexane
- trans
- metal hydroxide
- diisocyanate
- alkali metal
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- CDMDQYCEEKCBGR-UHFFFAOYSA-N 1,4-diisocyanatocyclohexane Chemical compound O=C=NC1CCC(N=C=O)CC1 CDMDQYCEEKCBGR-UHFFFAOYSA-N 0.000 title abstract 4
- 150000008044 alkali metal hydroxides Chemical class 0.000 abstract 4
- PXGZQGDTEZPERC-UHFFFAOYSA-N 1,4-cyclohexanedicarboxylic acid Chemical compound OC(=O)C1CCC(C(O)=O)CC1 PXGZQGDTEZPERC-UHFFFAOYSA-N 0.000 abstract 3
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 abstract 3
- 229910001860 alkaline earth metal hydroxide Inorganic materials 0.000 abstract 3
- LYCAIKOWRPUZTN-UHFFFAOYSA-N ethylene glycol Natural products OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 abstract 3
- 239000011541 reaction mixture Substances 0.000 abstract 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 abstract 2
- OAKJQQAXSVQMHS-UHFFFAOYSA-N Hydrazine Chemical compound NN OAKJQQAXSVQMHS-UHFFFAOYSA-N 0.000 abstract 2
- 239000004202 carbamide Substances 0.000 abstract 2
- VKIRRGRTJUUZHS-UHFFFAOYSA-N cyclohexane-1,4-diamine Chemical compound NC1CCC(N)CC1 VKIRRGRTJUUZHS-UHFFFAOYSA-N 0.000 abstract 2
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 abstract 2
- -1 trans-cyclohexane-1,4-disulphonyl urea Chemical compound 0.000 abstract 2
- XMKLTEGSALONPH-UHFFFAOYSA-N 1,2,4,5-tetrazinane-3,6-dione Chemical compound O=C1NNC(=O)NN1 XMKLTEGSALONPH-UHFFFAOYSA-N 0.000 abstract 1
- OLSJVTLNNWLLIL-UHFFFAOYSA-N 1,3-disulfonylurea Chemical compound O=S(=O)=NC(=O)N=S(=O)=O OLSJVTLNNWLLIL-UHFFFAOYSA-N 0.000 abstract 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 abstract 1
- 125000005907 alkyl ester group Chemical group 0.000 abstract 1
- 229910021529 ammonia Inorganic materials 0.000 abstract 1
- 150000001875 compounds Chemical class 0.000 abstract 1
- 150000002148 esters Chemical class 0.000 abstract 1
- 229910000041 hydrogen chloride Inorganic materials 0.000 abstract 1
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 abstract 1
- 239000012442 inert solvent Substances 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 229920000728 polyester Polymers 0.000 abstract 1
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 abstract 1
- 125000000467 secondary amino group Chemical class [H]N([*:1])[*:2] 0.000 abstract 1
- 239000007787 solid Substances 0.000 abstract 1
- FDDDEECHVMSUSB-UHFFFAOYSA-N sulfanilamide Chemical compound NC1=CC=C(S(N)(=O)=O)C=C1 FDDDEECHVMSUSB-UHFFFAOYSA-N 0.000 abstract 1
- 229940124530 sulfonamide Drugs 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C273/00—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
- C07C273/18—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of substituted ureas
- C07C273/1809—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of substituted ureas with formation of the N-C(O)-N moiety
- C07C273/1836—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of substituted ureas with formation of the N-C(O)-N moiety from derivatives of carbamic acid
- C07C273/1845—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of substituted ureas with formation of the N-C(O)-N moiety from derivatives of carbamic acid comprising the -N-C(O)-Hal moiety
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C311/00—Amides of sulfonic acids, i.e. compounds having singly-bound oxygen atoms of sulfo groups replaced by nitrogen atoms, not being part of nitro or nitroso groups
- C07C311/50—Compounds containing any of the groups, X being a hetero atom, Y being any atom
- C07C311/52—Y being a hetero atom
- C07C311/54—Y being a hetero atom either X or Y, but not both, being nitrogen atoms, e.g. N-sulfonylurea
- C07C311/56—Y being a hetero atom either X or Y, but not both, being nitrogen atoms, e.g. N-sulfonylurea having sulfur atoms of the sulfonylurea groups bound to carbon atoms of rings other than six-membered aromatic rings
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE2710595A DE2710595C3 (de) | 1977-03-11 | 1977-03-11 | Verfahren zur Herstellung der Trans-Isomeren von Cyclohexan-l,4-diamin-, diurethanen, -diharnstoffen, -disulfonylharnstoffen und -diisocyanat |
Publications (1)
Publication Number | Publication Date |
---|---|
ES466943A1 true ES466943A1 (es) | 1978-10-01 |
Family
ID=6003336
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ES466943A Expired ES466943A1 (es) | 1977-03-11 | 1978-02-14 | Procedimiento para la preparacion de trans-ciclohexan-1,4- diisocianato, transciclohexan,1,4-diamina,trans-ciclohexan- 1,4-diuretanos, trans-ciclohexan 1,4-diureas o de trans-ci- clohexan-1,4-disulfonilureas. |
Country Status (16)
Country | Link |
---|---|
US (7) | US4203916A (en]) |
JP (2) | JPS53112849A (en]) |
AT (1) | AT355010B (en]) |
AU (1) | AU519392B2 (en]) |
BE (1) | BE864741A (en]) |
BR (1) | BR7800560A (en]) |
CA (1) | CA1100522A (en]) |
DD (1) | DD132865A5 (en]) |
DE (1) | DE2710595C3 (en]) |
ES (1) | ES466943A1 (en]) |
FR (1) | FR2383169A1 (en]) |
GB (1) | GB1598666A (en]) |
IT (1) | IT1104132B (en]) |
NL (1) | NL7802232A (en]) |
SE (1) | SE7802752L (en]) |
SU (1) | SU841579A3 (en]) |
Families Citing this family (27)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE2829199A1 (de) * | 1978-07-03 | 1980-02-21 | Akzo Gmbh | Polyurethane aus trans-cyclohexan- 1,4-diisocyanat |
DE3233384A1 (de) * | 1982-09-08 | 1984-03-08 | Akzo Gmbh, 5600 Wuppertal | Thermoplastische polyurethan-elastomere aus cyclohexan-1.4-diisocyanat |
US4808471A (en) * | 1985-03-01 | 1989-02-28 | Minnesota Mining And Manufacturing Company | Flat transparent top coat for retroreflective sheeting |
DE3536017A1 (de) * | 1985-10-09 | 1987-04-09 | Huels Chemische Werke Ag | Ganz oder teilweise mit epsilon-caprolactam blockiertes trans-cyclohexan-1,4-diisocyanat, dessen herstellung und verwendung |
US4820830A (en) * | 1987-03-02 | 1989-04-11 | King Industries, Inc. | Certain hydroxyalkyl carbamates, polymers and uses thereof |
JPH01159897U (en]) * | 1988-04-28 | 1989-11-06 | ||
US5319133A (en) * | 1992-12-28 | 1994-06-07 | Olin Corporation | Isocyanates and their preparation using hypochlorous acid |
SE9802208D0 (sv) * | 1998-06-22 | 1998-06-22 | Astra Pharma Inc | Novel compounds |
DE19917961A1 (de) * | 1999-04-21 | 2000-10-26 | Degussa | Verfahren zur Herstellung von Aminosäurederivaten |
US7074803B2 (en) * | 2001-03-02 | 2006-07-11 | Durect Corporation | Opioid formulations |
KR100698813B1 (ko) * | 2000-04-03 | 2007-03-23 | 미쓰비시 가가꾸 가부시키가이샤 | 적층체, 접착 방법 및 활성 에너지선-경화성 조성물 |
JP2003064047A (ja) * | 2001-08-23 | 2003-03-05 | Tendou Seiyaku Kk | 新規シクロヘキサン誘導体、それを含有するオルガノゲル化剤及びオルガノゲル |
JP5692964B2 (ja) * | 2006-01-13 | 2015-04-01 | ビーエーエスエフ ソシエタス・ヨーロピアBasf Se | イソシアネートの製造法 |
WO2008088359A2 (en) * | 2006-12-20 | 2008-07-24 | Tom, Helen, Y. | Skate guards 'blinkerz' for figure and hockey skates blades |
EP2204395B1 (en) * | 2007-10-15 | 2013-10-09 | Mitsui Chemicals, Inc. | Polyurethane resin |
US20100227985A1 (en) | 2007-10-15 | 2010-09-09 | Mitsui Chemicals, Inc. | Granular polyurethane resin composition and molded article of the same |
CN101735111B (zh) * | 2009-12-31 | 2011-12-14 | 江苏恒祥化工有限责任公司 | 反式-1,4-环己烷二异氰酸酯的合成方法 |
US8871969B2 (en) | 2011-05-30 | 2014-10-28 | Basf Se | Process for the production of polyisocyanates |
US9328219B2 (en) | 2012-03-20 | 2016-05-03 | Basf Se | Polyamide compositions with improved optical properties |
BR112014022977B1 (pt) | 2012-03-20 | 2020-12-29 | Basf Se | composição polimérica, uso de um composto da fórmula i, artigo moldado e composto |
US8772527B2 (en) | 2012-04-27 | 2014-07-08 | Basf Se | Process for isomerization of cis-2-pentenenitrile to 3-pentenenitriles |
CN104364295A (zh) * | 2012-05-25 | 2015-02-18 | 帝斯曼知识产权资产管理有限公司 | 具有高熔融温度的可熔融加工的聚酰胺 |
EP2968347B1 (en) * | 2013-03-15 | 2023-08-02 | The Regents of the University of California | Modulators of the eif2alpha pathway |
JP7114109B2 (ja) * | 2017-10-05 | 2022-08-08 | ノボマー, インコーポレイテッド | イソシアネート、誘導体及びその製造方法 |
JP7021503B2 (ja) * | 2017-11-02 | 2022-02-17 | 三菱瓦斯化学株式会社 | 脂肪族ジアミンの製造方法 |
CN111315807B (zh) | 2017-12-18 | 2022-06-17 | 巴斯夫欧洲公司 | 具有改善的光学性能的聚酰胺模塑组合物及其中着色剂的用途 |
CN113563562B (zh) * | 2021-08-23 | 2022-05-13 | 无锡安睿驰科技有限公司 | 一种盘覆式自修复安全轮胎胶料及其制备方法 |
Family Cites Families (21)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2390165A (en) | 1940-11-07 | 1945-12-04 | Orthner Ludwig | Imine condensation process |
US2773086A (en) * | 1953-01-19 | 1956-12-04 | Monsanto Chemicals | Production of isocyanates from substituted ureas |
US2728787A (en) * | 1953-03-03 | 1955-12-27 | Rohm & Haas | Process for preparing organic diisocyanates |
US3151143A (en) * | 1959-09-04 | 1964-09-29 | Hooker Chemical Corp | Polyhalogen containing bicyclic dhsocyanates |
US3105848A (en) | 1960-05-02 | 1963-10-01 | Hooker Chemical Corp | Compounds 4-chloro-m-phenylene dimethyl carbamate and nu, nu'-dichloro isophthalamide |
US3167587A (en) * | 1961-12-28 | 1965-01-26 | Monsanto Co | Preparation of trans 1, 2-diamino-cyclohexane |
US3163675A (en) * | 1961-12-28 | 1964-12-29 | Monsanto Co | Preparation of trans 1, 2-diamino-cyclohexane |
US3187045A (en) * | 1961-12-28 | 1965-06-01 | Monsanto Co | Preparation of trans 1, 2-diaminocyclohexane |
US3296303A (en) * | 1963-08-23 | 1967-01-03 | Rohm & Haas | Method for the preparation of amides |
US3518307A (en) * | 1967-02-06 | 1970-06-30 | Geigy Chem Corp | Cyclohexenyl amines |
US3644459A (en) * | 1968-05-15 | 1972-02-22 | Mobay Chemical Corp | Isomeric mixtures of methylcyclohexylene diisocyanate |
US3880925A (en) * | 1969-10-31 | 1975-04-29 | Jr Arthur W Langer | Separation and purification of cis and trans isomers |
DE2129200B2 (de) * | 1971-06-12 | 1979-09-27 | Bayer Ag, 5090 Leverkusen | Verfahren zur Herstellung von N-A rj !harnstoffen |
US4082749A (en) * | 1973-06-06 | 1978-04-04 | Basf Aktiengesellschaft | Process for the production of amines |
DE2437470B2 (de) | 1974-08-03 | 1976-09-16 | Akzo Gmbh, 5600 Wuppertal | Verfahren zur herstellung von diamiden aromatischer und cycloaliphatischer dicarbonsaeuren |
US4288625A (en) * | 1974-08-22 | 1981-09-08 | Phillips Petroleum Co. | Dinitriles, diamines, and polyamides |
FR2298532A1 (fr) * | 1975-01-22 | 1976-08-20 | Akzo Nv | Bis-n-chloramides des acides carboxyliques aromatiques et cycloaliphatiques |
DE2502428C2 (de) | 1975-01-22 | 1976-11-18 | Akzo Gmbh | Verfahren zur herstellung von na- oder k-salzen von arylen- bis -sulfonylharnstoffen oder der entsprechenden arylenbis-sulfonylharnstoffen |
GB1604696A (en) * | 1977-04-26 | 1981-12-16 | Anic Spa | Dinitriles their production and their use in the production of diamines and polyamides |
DE2824648C2 (de) * | 1978-06-05 | 1982-06-24 | Akzo Gmbh, 5600 Wuppertal | Verfahren zur Herstellung von Isocyanaten |
DE3015374A1 (de) * | 1980-04-22 | 1981-10-29 | Akzo Gmbh, 5600 Wuppertal | Verfahren zur herstellung von harnstoffen |
-
1977
- 1977-03-11 DE DE2710595A patent/DE2710595C3/de not_active Expired
- 1977-12-21 AT AT918177A patent/AT355010B/de not_active IP Right Cessation
-
1978
- 1978-01-12 IT IT47615/78A patent/IT1104132B/it active
- 1978-01-30 BR BR7800560A patent/BR7800560A/pt unknown
- 1978-02-14 ES ES466943A patent/ES466943A1/es not_active Expired
- 1978-02-28 FR FR7805723A patent/FR2383169A1/fr active Granted
- 1978-03-01 NL NL7802232A patent/NL7802232A/xx not_active Application Discontinuation
- 1978-03-03 AU AU33826/78A patent/AU519392B2/en not_active Expired
- 1978-03-06 US US05/883,949 patent/US4203916A/en not_active Expired - Lifetime
- 1978-03-09 DD DD7800204069A patent/DD132865A5/xx unknown
- 1978-03-10 BE BE185800A patent/BE864741A/xx unknown
- 1978-03-10 SE SE7802752A patent/SE7802752L/xx unknown
- 1978-03-10 GB GB9536/78A patent/GB1598666A/en not_active Expired
- 1978-03-10 CA CA298,719A patent/CA1100522A/en not_active Expired
- 1978-03-10 JP JP2759778A patent/JPS53112849A/ja active Granted
-
1979
- 1979-03-06 SU SU792734749A patent/SU841579A3/ru active
- 1979-06-18 US US06/049,112 patent/US4275223A/en not_active Expired - Lifetime
-
1980
- 1980-12-11 US US06/215,415 patent/US4418211A/en not_active Expired - Lifetime
-
1982
- 1982-09-20 US US06/420,184 patent/US4439370A/en not_active Expired - Fee Related
- 1982-09-20 US US06/420,185 patent/US4457871A/en not_active Expired - Fee Related
- 1982-09-20 US US06/420,186 patent/US4486603A/en not_active Expired - Fee Related
- 1982-09-20 US US06/420,187 patent/US4467114A/en not_active Expired - Fee Related
-
1987
- 1987-01-29 JP JP62017435A patent/JPS62246547A/ja active Granted
Also Published As
Publication number | Publication date |
---|---|
AU3382678A (en) | 1979-09-06 |
BR7800560A (pt) | 1978-10-03 |
JPS638097B2 (en]) | 1988-02-19 |
DD132865A5 (de) | 1978-11-15 |
NL7802232A (nl) | 1978-09-13 |
US4203916A (en) | 1980-05-20 |
DE2710595B2 (de) | 1980-03-13 |
JPS6229425B2 (en]) | 1987-06-25 |
DE2710595C3 (de) | 1980-11-06 |
FR2383169B1 (en]) | 1982-12-17 |
DE2710595A1 (de) | 1978-09-14 |
SU841579A3 (ru) | 1981-06-23 |
JPS62246547A (ja) | 1987-10-27 |
US4439370A (en) | 1984-03-27 |
CA1100522A (en) | 1981-05-05 |
JPS53112849A (en) | 1978-10-02 |
US4418211A (en) | 1983-11-29 |
GB1598666A (en) | 1981-09-23 |
AT355010B (de) | 1980-02-11 |
IT7847615A0 (it) | 1978-01-12 |
US4467114A (en) | 1984-08-21 |
US4275223A (en) | 1981-06-23 |
FR2383169A1 (fr) | 1978-10-06 |
US4457871A (en) | 1984-07-03 |
IT1104132B (it) | 1985-10-14 |
BE864741A (fr) | 1978-07-03 |
US4486603A (en) | 1984-12-04 |
AU519392B2 (en) | 1981-12-03 |
ATA918177A (de) | 1979-07-15 |
SE7802752L (sv) | 1978-09-12 |
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